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Produktbild: Basic Gas Chromatography

Basic Gas Chromatography

Fr. 104.00

inkl. gesetzl. MwSt., Versandkostenfrei

Beschreibung

Produktdetails

Einband

Gebundene Ausgabe

Erscheinungsdatum

10.06.2009

Verlag

John Wiley & Sons Inc

Seitenzahl

256

Maße (L/B/H)

24/16.1/1.8 cm

Gewicht

544 g

Auflage

2. Auflage

Sprache

Englisch

ISBN

978-0-470-43954-8

Beschreibung

Rezension

"The book should appeal to readers with varying levels of education and emphasises a practical, applied approach to the subject. Basic Gas Chromatography, 2nd Edition remains the standard handbook for everyone from undergraduates studying analytical chemistry to working industrial chemists. It is particularly suited for intensive short courses." (Chemistry Journals, 11 April 2011)

Produktdetails

Einband

Gebundene Ausgabe

Erscheinungsdatum

10.06.2009

Verlag

John Wiley & Sons Inc

Seitenzahl

256

Maße (L/B/H)

24/16.1/1.8 cm

Gewicht

544 g

Auflage

2. Auflage

Sprache

Englisch

ISBN

978-0-470-43954-8

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  • Produktbild: Basic Gas Chromatography
  • PREFACE TO THE SECOND EDITION.

    PREFACE.

    ACKNOWLEDGMENTS.

    1 INTRODUCTION.

    A Brief History.

    Definitions.

    Overview: Advantages and Disadvantages.

    Instrumentation.

    References.

    2 INSTRUMENT OVERVIEW.

    Carrier Gas.

    Flow Control and Measurement.

    Sample Inlets and Sampling Devices.

    Columns.

    Temperature Zones.

    Detectors.

    Data Systems.

    References.

    3 BASIC CONCEPTS AND TERMS.

    Definitions, Terms, and Symbols.

    The Rate Theory.

    A Redefinition of H.

    The Achievement of Separation.

    References.

    4 STATIONARY PHASES.

    Selecting a Column.

    Classification of Stationary Phases for GLC.

    Liquid Stationary Phases (GLC).

    Solid Stationary Phases (GSC).

    References.

    5 PACKED COLUMNS AND INLETS.

    Solid Supports.

    Liquid Stationary Phases.

    Solid Stationary Phases (GSC).

    Gas Analysis.

    Analysis of Other Inorganics.

    Inlets for Liquid Samples and Solutions.

    Special Columns.

    Upgrading for Capillary Columns.

    References.

    6 CAPILLARY COLUMNS AND INLETS.

    Types of OT Columns.

    OT Column Tubing.

    Advantages of OT Columns.

    Column Selection.

    Capillary Inlet Systems.

    Miscellaneous Topics.

    References.

    7 DETECTORS.

    Classification of Detectors.

    Detector Characteristics.

    Flame Ionization Detector (FID).

    Thermal Conductivity Detector (TCD).

    Electron Capture Detector (ECD).

    Other Detectors.

    References.

    8 QUALITATIVE AND QUANTITATIVE ANALYSIS.

    Qualitative Analysis.

    Quantitative Analysis.

    References.

    9 PROGRAMMED TEMPERATURE.

    Temperature Effects.

    Advantages and Disadvantages of PTGC.

    Requirements of PTGC.

    Theory of PTGC.

    Special Topics.

    References.

    10 GAS CHROMATOGRAPHY-MASS SPECTROMETRY (GC-MS).

    Instrumentation.

    History.

    Limitations of GC-MS Systems.

    Data Analysis.

    References.

    11 MULTIDIMENSIONAL GAS CHROMATOGRAPHY.

    Overview.

    Fundamental Principles of Multidimensional Chromatography.

    GC×GC with Heart Cutting.

    Comprehensive GC×GC.

    LC×GC with Heart Cutting.

    Comprehensive LC×GC.

    Summary.

    References.

    12 SAMPLING METHODS.

    Overview.

    Liquid-Liquid Extraction (LLE).

    Solid-Liquid Extraction: Soxhlet Extraction and Accelerated Solvent Extraction (ASE).

    Liquid-Solid Extraction: Solid-Phase Extraction (SPE).

    Liquid- or Solid-Vapor Extraction: Headspace Extraction.

    Solid-Phase Micro-extraction (SPME).

    Additional Techniques and Summary.

    References.

    13 SPECIAL TOPICS.

    Fast GC.

    Chiral Analysis by GC.

    GC Analysis of Nonvolatile Compounds.

    References.

    14 TROUBLESHOOTING GC SYSTEMS.

    APPENDIX I SYMBOLS AND ACRONYMS.

    APPENDIX II GUIDELINES FOR SELECTING CAPILLARY COLUMNS.

    APPENDIX III GC: HOW TO AVOID PROBLEMS.

    APPENDIX IV CALCULATION OF SPLIT RATIO FOR SPLIT INJECTION ON OT COLUMNS.

    APPENDIX V OPERATING CONDITIONS FOR CAPILLARY COLUMNS.

    APPENDIX VI OV LIQUID PHASES PHYSICAL PROPERTY DATA.

    APPENDIX VII SOME COMPRESSIBILITY CORRECTION FACTORS (J).

    APPENDIX VIII SOME INTERNET WEBSITES FOR GAS CHROMATOGRAPHERS.

    APPENDIX IX OTHER BOOKS ON GAS CHROMATOGRAPHY.

    INDEX OF APPLICATIONS.

    INDEX.