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Produktbild: Portable Spectroscopy and Spectrometry, Technologies and Instrumentation

Portable Spectroscopy and Spectrometry, Technologies and Instrumentation Volume 1: Technologies and Instrumentation

Fr. 223.00

inkl. gesetzl. MwSt., Versandkostenfrei

Beschreibung

Produktdetails

Einband

Gebundene Ausgabe

Erscheinungsdatum

19.04.2021

Herausgeber

Richard A. Crocombe + weitere

Verlag

John Wiley & Sons

Seitenzahl

608

Maße (L/B/H)

26/20.6/3.7 cm

Gewicht

1418 g

Auflage

Volume 1 edition

Sprache

Englisch

ISBN

978-1-119-63636-6

Beschreibung

Produktdetails

Einband

Gebundene Ausgabe

Erscheinungsdatum

19.04.2021

Herausgeber

Verlag

John Wiley & Sons

Seitenzahl

608

Maße (L/B/H)

26/20.6/3.7 cm

Gewicht

1418 g

Auflage

Volume 1 edition

Sprache

Englisch

ISBN

978-1-119-63636-6

Herstelleradresse

Libri GmbH
Europaallee 1
36244 Bad Hersfeld
DE

Email: gpsr@libri.de

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  • Produktbild: Portable Spectroscopy and Spectrometry, Technologies and Instrumentation

  • List of Contributors xiii

    Foreword xvii

    Preface for Volume 1 xix

    Acknowledgements xxi

    1 Introduction to Portable Spectroscopy 1
    Pauline E. Leary, Richard A. Crocombe and Brooke W. Kammrath

    1.1 Introduction 1

    1.2 Defining Portable Spectrometers 1

    1.3 Performance 2

    1.4 History and Availability 4

    1.5 Instrument Design and Enabling Technologies 7

    1.6 Producing Results 8

    1.7 Outline of These Volumes 9

    Acronyms and Abbreviations 11

    References 12

    2 Engineering Portable Instruments 15
    Terry Sauer

    2.1 Size/Weight 15

    2.2 Sample Interface 16

    2.3 Embedded Computer vs. External Personal Computer (PC) 16

    2.4 Reduced Feature Set 17

    2.5 Target of Non-Spectroscopist 17

    2.6 Power Budget 18

    2.7 Voltage Conversion 18

    2.8 Decon/Ingress Protection (IP) Rating 19

    2.9 Testing the Seal 20

    2.10 Gloved Operation 20

    2.11 Display 21

    2.12 Thermal Concerns 23

    2.13 Optical Elements 27

    2.14 Interferometer Optical Design 27

    2.15 Interferometer Bearings 29

    2.16 Vibration 30

    2.17 Shock 30

    2.18 Battery 31

    2.19 Electrostatic Discharge (ESD) 32

    2.20 Ergonomics 34

    2.21 Laser Safety 34

    2.22 Stability 35

    2.23 Service 38

    2.24 Communications/Wireless 38

    References 38

    3 Design Considerations for Portable Mid-Infrared FTIR Spectrometers Used for In-Field Identifications of Threat Materials 41
    David W. Schiering and John T. Stein

    3.1 Introduction and Background 41

    3.2 FTIR System Components 44

    3.3 FTIR Spectrometer Performance Attributes 53

    3.4 Modeling and Simulation Guide to Portable Instrument Design and Development 55

    3.5 Portable FTIR Performance Benchmarks 60

    3.6 Conclusion 62

    Abbreviations and Acronyms 62

    References 63

    4 PAT Applications of NIR Spectroscopy in the Pharmaceutical Industry 67
    Pierre-Yves Sacré, Charlotte De Bleye, Philippe Hubert and Eric Ziemons

    4.1 Introduction 67

    4.2 Continuous Manufacturing and Real-Time Release Testing 67

    4.3 PAT Implementation of Near-Infrared Spectroscopy 73

    4.4 Conclusion 79

    Glossary 81

    References 82

    5 MOEMS and MEMS - Technology, Benefits & Uses 89
    Heinrich Grüger

    5.1 Introduction 89

    5.2 Grating-Based Spectrometers 92

    5.3 Fourier Transform Spectrometer 101

    5.4 Tunable Fabry-Perot Interferometer 104

    5.5 Integration Strategies for MEMS-/MOEMS-Based Spectrometers 106

    5.6 Use of MEMS-Based NIR Spectrometers 108

    Acronyms and Abbreviations 109

    References 110

    6 Portable Raman Spectroscopy: Instrumentation and Technology 115
    Cicely Rathmell, Dieter Bingemann, Mark Zieg and David Creasey

    6.1 Introduction 115

    6.2 The Case for Raman: Capabilities and Scope 115

    6.3 The Theory of Raman Spectra 116

    6.4 Basics of a Raman System 119

    6.5 "Portable" Versus "Handheld" Versus "Mini" 119

    6.6 Performance Needs in Portable Raman Instruments 120

    6.7 Excitation Laser 122

    6.8 Optical Filters and Sampling Optics 125

    6.9 Spectrometer Design 127

    6.10 Sample Interface and Accessories 134

    6.11 Spectral Processing and Analysis 135

    6.12 Special Cases 138

    6.13 Conclusion 140

    Acronyms and Abbreviations 141

    References 141

    7 Optical Filters - Technology and Applications 147
    Oliver Pust

    7.1 Overview on the Use of Optical Filters in Spectroscopy 147

    7.2 Optical Filters as Auxiliary Filters 154

    7.3 Optical Filters as Complementary Filters 159

    7.4 Optical Filters asWavelength Selective Element 161

    7.5 Conclusion and Outlook 175

    References 176

    8 Portable UV-Visible Spectroscopy - Instrumentation, Technology, and Applications 179
    Anshuman Das

    8.1 Introduction 179

    8.2 Typical Instrumentation of a Portable UV-Vis Spectrometer 180

    8.3 Measurement Configurations 183

    8.4 Types of Instrumentation Used in UV-Vis Spectroscopy 187

    8.5 Applications 193

    8.6 Challenges for Portable Spectrometers 202

    8.7 Outlook 204

    References 204

    9 Smartphone Technology - Instrumentation and Applications 209
    Alexander Scheeline

    9.1 Introduction and Context 209

    9.2 Challenges of Smartphone Spectrometry 210

    9.3 Progress to Date 213

    9.4 Conclusion and Prospective 230

    References 230

    10 Portable Standoff Optical Spectroscopy for Safety and Security 237
    Matthew P. Nelson and Nathaniel R. Gomer

    10.1 Introduction 237

    10.2 Portable Standoff Optical Instrument Types 240

    10.3 Portable Standoff Optical Instrument Technologies 242

    10.4 Portable Standoff Optical Spectroscopy Sensor Selection 248

    10.5 Portable Standoff Optical Spectroscopy Sensors and Applications 253

    10.6 Conclusions and Future Direction 269

    Acronyms and Abbreviations 269

    References 270

    11 Microplasmas for Portable Optical Emission Spectrometry 275
    Vassili Karanassios

    11.1 Introduction 275

    11.2 A Brief Review of the Portable Microplasma Literature 276

    11.3 Conclusion 284

    Acronyms 284

    Abbreviations 284

    Acknowledgments 285

    References 285

    12 Portable Electro-Optical-Infrared Spectroscopic Sensors for Standoff Detection of Chemical Leaks and Threats 289
    Hugo Lavoie, Jean-Marc Thériault, Eldon Puckrin, Richard L. Lachance, Alexandre Thibeault, Yotam Ariel and Jean Albert

    12.1 Introduction 289

    12.2 A Differential FTIR Approach for Standoff Gas Detection 289

    12.3 iCATSI Sensor 297

    12.4 Active FTIR for Ground Contamination Detection 299

    12.5 Signature Collection: Broadband Portable Field Spectral Reflectometer 303

    12.6 Imaging Gas Filter Correlation Radiometry 308

    12.7 Conclusion 317

    References 317

    13 Handheld Laser Induced Breakdown Spectroscopy (HHLIBS) 321
    David Day

    13.1 Introduction 321

    13.2 Handheld LIBS-Enabling Technologies 323

    13.3 Commercial HHLIBS Specifications 337

    13.4 HHLIBS Applications 337

    13.5 Summary and Future Expectations 341

    References 341

    14 Miniaturized Mass Spectrometry - Instrumentation, Technology, and Applications 345
    Dalton T. Snyder

    14.1 Introduction 345

    14.2 Instrumentation 346

    14.3 Applications 358

    14.4 Summary and Outlook 364

    Acronyms 364

    Further Reading 365

    15 Portable Gas Chromatography-Mass Spectrometry: Instrumentation and Applications 367
    Pauline E. Leary, Brooke W. Kammrath and John A. Reffner

    15.1 Introduction 367

    15.2 History of Portable GC-MS 368

    15.3 Critical Components for Portability 370

    15.4 Applications 379

    15.5 The Future of Portable GC-MS 384

    Acknowledgments 385

    References 385

    16 Development of High-Pressure Mass Spectrometry for Handheld and Benchtop Analyzers 391
    Kenion H. Blakeman and Scott E. Miller

    16.1 Introduction 391

    16.2 Ion Trap Development for HPMS 392

    16.3 Commercialization and Applications 401

    16.4 Conclusions 408

    References 408

    17 Key Instrumentation Developments That Have Led to Portable Ion Mobility Spectrometer Systems 415
    Reno F. DeBono and Pauline E. Leary

    17.1 Background and History 415

    17.2 Principles of Ion Mobility Spectrometry 417

    17.3 Current Innovations and Future Directions 439

    17.4 Conclusions 441

    Acronyms 442

    Abbreviations and Symbols 443

    References 444

    18 X-Ray Sources for Handheld X-Ray Fluorescence Instruments 449
    Sterling Cornaby

    18.1 Background 449

    18.2 The Miniature X-Ray Source 450

    18.3 The Selection of a Target Anode Material for XRF 455

    18.4 Functionality of X-Ray Sources for HHXRF 461

    18.5 Conclusion 472

    References 473

    19 Semiconductor Detectors for Portable Energy-Dispersive XRF Spectrometry 475
    Andrei Stratilatov

    19.1 Introduction 475

    19.2 Semiconductor Detector Fundamentals: Signal Formation 476

    19.3 Detectors for Portable Spectrometers: Design and Performance 486

    19.4 Silicon Drift Detectors 489

    19.5 Si Detectors' Quantum Efficiency: X-Ray EntranceWindows 491

    19.6 Conclusion 498

    Acronyms and Abbreviations 499

    References 499

    20 Field-Deployable Utility of Benchtop Nuclear Magnetic Resonance Spectrometers 501
    Koby L. Kizzire and Griffin Cassata

    20.1 Introduction 501

    20.2 NMR Theory 503

    20.3 Magnet Miniaturization 505

    20.4 Improvements in Sensitivity and Resolution 506

    20.5 Current bNMR Spectrometers 507

    20.6 Applications 509

    20.7 Conclusion 510

    References 511

    21 Rapid DNA Analysis - Need, Technology, and Applications 515
    Claire L. Glynn and Angie Ambers

    21.1 Need for Speed 515

    21.2 Technology 518

    21.3 Applications 529

    21.4 Limitations and Important Considerations 538

    21.5 Future Considerations and Conclusions 539

    A Appendix 540

    A.1 Acronyms 540

    References 541

    22 Portable Biological Spectroscopy: Field Applications 545
    Brian Damit and Miquel Antoine

    22.1 Introduction 545

    22.2 Organization of This Chapter 547

    22.3 Attributes of Field-Portable Spectroscopy Systems 547

    22.4 Field Applications 548

    22.5 Summary, Challenges, and Outlook 558

    Acknowledgements 558

    List of Acronyms 559

    References 559

    Index 565