Produktbild: Understanding NMR Spectroscopy

Understanding NMR Spectroscopy

Fr. 239.00

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Beschreibung

Produktdetails

Einband

Gebundene Ausgabe

Erscheinungsdatum

29.09.2010

Verlag

John Wiley & Sons

Seitenzahl

526

Maße (L/B/H)

3.1/18.9/24.6 cm

Gewicht

1426 g

Auflage

2. Auflage

Sprache

Englisch

ISBN

978-0-470-74609-7

Beschreibung

Produktdetails

Einband

Gebundene Ausgabe

Erscheinungsdatum

29.09.2010

Verlag

John Wiley & Sons

Seitenzahl

526

Maße (L/B/H)

3.1/18.9/24.6 cm

Gewicht

1426 g

Auflage

2. Auflage

Sprache

Englisch

ISBN

978-0-470-74609-7

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  • Produktbild: Understanding NMR Spectroscopy
  • Preface.
     
    Preface to the first edition.
     
    1 What this book is about and who should read it.
     
    1.1 How this book is organized.
     
    1.2 Scope and limitations.
     
    1.3 Context and further reading.
     
    1.4 On-line resources.
     
    1.5 Abbreviations and acronyms.
     
    2 Setting the scene.
     
    2.1 NMR frequencies and chemical shifts.
     
    2.2 Linewidths, lineshapes and integrals.
     
    2.3 Scalar coupling.
     
    2.4 The basic NMR experiment.
     
    2.5 Frequency, oscillations and rotations.
     
    2.6 Photons.
     
    2.7 Further reading.
     
    2.8 Exercises.
     
    3 Energy levels and NMR spectra.
     
    3.1 The problem with the energy level approach.
     
    3.2 Introducing quantum mechanics.
     
    3.3 The spectrum from one spin.
     
    3.4 Writing the Hamiltonian in frequency units.
     
    3.5 The energy levels for two coupled spins.
     
    3.6 The spectrum from two coupled spins.
     
    3.7 Three spins.
     
    3.8 Further reading.
     
    3.9 Exercises.
     
    4 The vector model.
     
    4.1 The bulk magnetization.
     
    4.2 Larmor precession.
     
    4.3 Detection.
     
    4.4 Pulses.
     
    4.5 On-resonance pulses.
     
    4.6 Detection in the rotating frame.
     
    4.7 The basic pulse-acquire experiment.
     
    4.8 Pulse calibration.
     
    4.9 The spin echo.
     
    4.10 Pulses of different phases.
     
    4.11 Off-resonance effects and soft pulses.
     
    4.12 Further reading.
     
    4.13 Exercises.
     
    5 Fourier transformation and data processing.
     
    5.1 How the Fourier transform works.
     
    5.2 Representing the FID.
     
    5.3 Lineshapes and phase.
     
    5.4 Manipulating the FID and the spectrum.
     
    5.5 Zero filling.
     
    5.6 Truncation.
     
    5.7 Further reading.
     
    5.8 Exercises.
     
    6 The quantum mechanics of one spin.
     
    6.1 Introduction.
     
    6.2 Superposition states.
     
    6.3 Some quantum mechanical tools.
     
    6.4 Computing the bulk magnetization.
     
    6.5 Time evolution.
     
    6.6 RF pulses.
     
    6.7 Making faster progress: the density operator.
     
    6.8 Coherence.
     
    6.9 Further reading.
     
    6.10 Exercises.
     
    7 Product operators.
     
    7.1 Operators for one spin.
     
    7.2 Analysis of pulse sequences for a one-spin system.
     
    7.3 Speeding things up.
     
    7.4 Operators for two spins.
     
    7.5 In-phase and anti-phase terms.
     
    7.6 Hamiltonians for two spins.
     
    7.7 Notation for heteronuclear spin systems.
     
    7.8 Spin echoes and J-modulation.
     
    7.9 Coherence transfer.
     
    7.10 The INEPT experiment.
     
    7.11 Selective COSY.
     
    7.12 Coherence order and multiple-quantum coherences.
     
    7.13 Further reading.
     
    7.14 Exercises.
     
    8 Two-dimensional NMR.
     
    8.1 The general scheme for two-dimensional NMR.
     
    8.2 Modulation and lineshapes.
     
    8.3 COSY.
     
    8.4 Double-quantum filtered COSY (DQF COSY).
     
    8.5 Double-quantum spectroscopy.
     
    8.6 Heteronuclear correlation spectra.
     
    8.7 HSQC.
     
    8.8 HMQC.
     
    8.9 Long-range correlation: HMBC.
     
    8.10 HETCOR.
     
    8.11 TOCSY.
     
    8.12 Frequency discrimination and lineshapes.
     
    8.13 Further reading.
     
    8.14 Exercises.
     
    9 Relaxation and the NOE.
     
    9.1 The origin of relaxation.
     
    9.2 Relaxation mechanisms.
     
    9.3 Describing random motion - the correlation time.
     
    9.4 Populations.
     
    9.5 Longitudinal relaxatio