• Produktbild: Chemical Derivatization in Analytical Chemistry
  • Produktbild: Chemical Derivatization in Analytical Chemistry
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Chemical Derivatization in Analytical Chemistry Chromatography

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Beschreibung

Produktdetails

Einband

Taschenbuch

Erscheinungsdatum

24.12.2012

Herausgeber

R. W. Frei

Verlag

Springer Us

Seitenzahl

344

Maße (L/B/H)

23.5/15.5/2 cm

Gewicht

546 g

Auflage

Softcover reprint of the original 1st ed. 1981

Sprache

Englisch

ISBN

978-1-4615-9196-2

Beschreibung

Produktdetails

Einband

Taschenbuch

Erscheinungsdatum

24.12.2012

Herausgeber

R. W. Frei

Verlag

Springer Us

Seitenzahl

344

Maße (L/B/H)

23.5/15.5/2 cm

Gewicht

546 g

Auflage

Softcover reprint of the original 1st ed. 1981

Sprache

Englisch

ISBN

978-1-4615-9196-2

Herstelleradresse

Springer-Verlag KG
Sachsenplatz 4-6
1201 Wien
AT

Email: GPSR Kontakt

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  • Produktbild: Chemical Derivatization in Analytical Chemistry
  • Produktbild: Chemical Derivatization in Analytical Chemistry
  • 1. Chemical Derivatization in Pesticide Analysis.- 1. Introduction.- 2. Organochlorine Insecticides.- 2.1. The DDT Group.- 2.2. Cyclodiene Insecticides.- 2.3. Miscellaneous.- 2.4. Cleanup Techniques Using Chemical Reactions.- 3. Organophosphorus Insecticides.- 3.1. Derivatization of the P Moiety.- 3.2. Derivatization of the Alkyl or Aryl Moiety.- 3.3. On-Column Transesterification.- 3.4. Derivatization of the Intact Insecticide.- 4. Carbamates (Insecticides and Herbicides).- 4.1. Hydrolysis and Derivatization of the N Moiety.- 4.2. Hydrolysis and Derivatization of the Alkyl or Aryl Moiety.- 4.3. On-Column Methylation.- 4.4. Derivatization of the Intact Carbamate.- 5. Herbicides.- 5.1. Triazines.- 5.2. Ureas.- 5.3. Chlorophenoxy Acids.- 5.4. Miscellaneous.- 6. Phenols.- 7. Fungicides.- References.- 2. Cyclic Boronates as Derivatives for the Gas Chromatography—Mass Spectrometry of Bifunctional Organic Compounds.- 1. Introduction.- 2. Some Historical Background.- 3. The Scope of Application of Cyclic Boronates in Gas Chromatography.- 4. Gas Chromatographic Properties of Cyclic Boronates.- 5. Mass Spectrometric Properties of Cyclic Boronates.- 6. Preparation of Cyclic Boronates for Use in Gas Chromatography-Mass Spectrometry.- 7. Examples of the Preparation and Gas Chromatography of Cyclic Boronates...- 8. Summary.- References.- 3. General Aspects of Precolumn Derivatization with Emphasis on Pharmaceutical Analysis.- 1. Introduction.- 1.1. Purposes for Derivatization.- 1.2. HPLC Detectors and Compatible Derivatives.- 1.3. Chemical Reactions Used in Derivatization.- 2. Functional Group Analysis.- 2.1. Amines.- 2.2. Alcohols and Phenols.- 2.3. Carboxylic Acids.- 2.4. Aldehydes and Ketones.- 2.5. Miscellaneous Nitrogen-Containing Compounds.- 2.6. Thiols.- 3. Detector Amplification by Paired Ion Chromatography.- 3.1. Theoretical Considerations.- 3.2. Applications.- 4. Conclusions.- References.- 4. Reaction Detectors in Liquid Chromatography.- 1. Introduction.- 2. Theoretical Aspects.- 2.1 Tubular Reactors.- 2.1. Bed Reactors.- 2.2. Segmented Stream Reactors.- 2.3. Mixing Units.- 3. Technical Aspects and Applications.- 3.1. Tubular Reactors (Nonsegmented Streams).- 3.2. Bed Reactors.- 3.3. Segmented Stream Reactors.- 4. Special Applications and Trends.- 4.1. Coupling with Other Detection Modes.- 4.2. Coupling with Other Techniques.- 5. Conclusions.- References.